As the pet food market has diversified away from traditional dry kibble or canned pet food options, pet parents have never had more variety in pet food product forms to choose from. Of these new forms, freeze-dried products and the fresh/frozen category have seen tremendous growth over the past few years. Both styles are marketed as minimally processed and healthier for pets than traditional dry kibble. Freeze-dried diets and treats are not extruded or subjected to extreme processing, and sometimes may be referred to as raw. Fresh and frozen diets have existed since 2006, but they have increasingly gained popularity. In recent years there has been strong growth of fresh human foods, through home delivery services with $16 billion revenue in 20221. This is followed by emerging growth in fresh, home delivered pet diets with an estimated value of $9 billion by 20302. Fresh and freeze-dried products represent the extremes of percent moisture, fat level, and storage temperature and provide unique challenges for preservation. The approaches to preserve each and achieve shelf-life requirements have evolved in recent years to address these challenges.
Preserving Freeze-Dried Pet Food
What freeze-dried products lack in weight, they make up for in flavor impact and texture. The high degree of palatability of freeze-dried products for cats makes them particularly appealing alone or as a topper for kibble. Making freeze-dried products for pets typically starts with a fresh meat slurry, blending in any other formula ingredients, freezing rapidly to the product’s triple point, then forcing the loss of water through sublimation under vacuum or lyophilization.
Preservation of freeze-dried products to prevent microbial contamination is simple, because the water activity is too low to support microbial growth. Raw material quality is the most important factor in oxidation and off aromas due to lipid oxidation and biogenic amines formation. Raw meat slurry has a water activity suitable for microbial growth. Microbial growth at high levels, even when the slurry is held at refrigerated temperatures, can lead to formation of biogenic amines. Biogenic amines, such as histamine, tyramine, cadaverine and putrescine, survive processing and cause negative palatability impacts. Treatment of the meat slurry with antimicrobial additives extends the shelf-life of the slurry and prevents the formation of biogenic amines. High pressure pasteurization or irradiation may be used to prevent cross contamination during processing before packaging as well. When used as a kill step or when the microbial burden is so high that it requires extensive sterilization processes, oxidation can occur (see Figure 1).